With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.2382-96-9,Benzo[d]oxazole-2-thiol,as a common compound, the synthetic route is as follows.
General procedure: To a suspension of polyvinylpolypyrrolidone-supported hydrogen peroxide (0.175 g),silica sulfuric acid (0.1 g) and potassium iodide (0.02 mmol) in dichloromethane or ethylacetate (5 mL) was added a thiol (1 mmol), and the mixture was stirred at room temperaturefor the specified time (Table I). The progress of the reaction was monitored by TLC. Aftercompletion of the reaction, the reaction mixture was filtered and the residue washed withCH2Cl2 (20 mL), (the residue of entry 5 was washed with ethanol). Finally, the organicsolvent was evaporated and pure product was obtained as judged by TLC and 1H-NMRspectroscopy., 2382-96-9
As the paragraph descriping shows that 2382-96-9 is playing an increasingly important role.
Reference£º
Article; Ghorbani-Choghamarani, Arash; Nikoorazm, Mohsen; Azadi, Gouhar; Journal of the Serbian Chemical Society; vol. 78; 2; (2013); p. 173 – 178;,
Benzoxazole – Wikipedia
Benzoxazole | C7H5NO – PubChem