Some tips on 864274-04-4

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864274-04-4,864274-04-4, 2-Methylbenzo[d]oxazole-6-carbaldehyde is a benzoxazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

To the solution of rhodanine (1.21 g, 10 mmol) in ethanol (50 ml.) was added 2- methyl-benzooxazole-6-carbaldehyde (1.61 mg, 10 mmol, 1 eq) followed by pyridine (1 ml_). The reaction mixture was refluxed for 24 hours cooled to the room temperature. Solid was filtered to give 1.3 g (47 percent yield) of pure 5-(2-methyl- benzooxazol-6-ylmethylene)-2-thioxo-thiazolidin-4-one. 1H-NMR (DMSO): D2.67 (s, 3H), 2.85 (s, 3H), 7.66 (dd, 1 H, J=8.3 Hz, J’=1.7 Hz), 7.82 (d, 1 H, J=8.3 Hz), 8.00 (s, 1 H), 8.02 (d, 1 H, J=1.7 Hz). LC MS (m/e) = 277.0 (MH+). Rt = 2.02 min

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Reference£º
Patent; SMITHKLINE BEECHAM CORPORATION; WO2007/103755; (2007); A2;,
Benzoxazole – Wikipedia
Benzoxazole | C7H5NO – PubChem