Analyzing the synthesis route of 864274-04-4

864274-04-4 2-Methylbenzo[d]oxazole-6-carbaldehyde 21333989, abenzoxazole compound, is more and more widely used in various.

864274-04-4, 2-Methylbenzo[d]oxazole-6-carbaldehyde is a benzoxazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

To the solution of 2-(2,6-difluoro-phenylimino)-thiazolidin-4-one (105 mg, 0.5 mmol) in ethanol (5 mL) was added 2-methyl-benzooxazole-6-carbaldehyde (80 mg, 0.5 mmol, 1 eq) followed by piperidine (0.1 mL). The reaction mixture was refluxed for 48 hours and diethyl ether (3 mL) was added. Solid was filtered to give 58 mg (33 percent yield) of pure 2-(2-fluoro-phenylimino)-5-(2-methyl-benzooxazol-6-yl-methylene)- thiazolidin-4-one. LC MS (m/e) = 354.2 (MH+). Rt = 2.11 min.

864274-04-4 2-Methylbenzo[d]oxazole-6-carbaldehyde 21333989, abenzoxazole compound, is more and more widely used in various.

Reference£º
Patent; SMITHKLINE BEECHAM CORPORATION; WO2007/103755; (2007); A2;,
Benzoxazole – Wikipedia
Benzoxazole | C7H5NO – PubChem