New Advances in Chemical Research in 2021.The dynamic chemical diversity of the numerous elements, ions and molecules that constitute the basis of life provides wide challenges and opportunities for research. 75178-96-0, Name is tert-Butyl (3-aminopropyl)carbamate, molecular formula is , belongs to benzoxazole compound. In a document, author is Shagun, L. G., Application In Synthesis of tert-Butyl (3-aminopropyl)carbamate.
Reaction of 2-sulfanylbenzoxazole with 1-iodopropan-2-one, 2-iodo-1-phenylethanone, and 2-iodo-1-(thiophen-2-yl)ethanone without solvent and bases afforded bis(benzoxazol-2-yl)disulfonium derivatives in a single preparative stage. The reaction proceeds as a domino-process and includes the alkylation of a sulfanyl group of benzoxazole, the reduction of iodoketone with hydrogen iodide, the oxidation of 2-sulfanylbenzoxazole to disulfide, the alkylation of disulfide atoms of sulfur, and the formation of triiodideanions. The yield of disulfonium derivatives increases twice in the presence of equimolar amount of iodine.
A reaction mechanism is the microscopic path by which reactants are transformed into products. Each step is an elementary reaction. In my other articles, you can also check out more blogs about 75178-96-0. Application In Synthesis of tert-Butyl (3-aminopropyl)carbamate.
Reference:
Benzoxazole – Wikipedia,
,Benzoxazole | C7H5NO – PubChem